The Institute of Organic Chemistry has various devices and techniques at its disposal.

NMR tube in sample holder
TUBAF

Nuclear magnetic resonance spectroscopy and mass spectrometry

  • LC-SPE-NMR-MS instrument system (Liquid Chromatography - Solid Phase Extraction - Nuclear Magnetic Resonance Spectroscopy - Mass Spectrometry)

Coupled instrument system consisting of

  • Agilent Technologies Infinity II HPLC
  • JEOL AccuTOF 4G LC-Plus mass spectrometer (incl. additional dart ion source)
  • Chromtech PAL RTC solid phase extraction system
  • JEOL Resonance ECZ500R NMR spectrometer
  • . additional dart ion source)
  • Chromtech PAL RTC solid phase extraction system
  • JEOL Resonance ECZ500R NMR spectrometer (500 MHz)
  • HPLC-MS instrument system

Bruker amaZon SL (ESI and APCI) coupled with

  • Dionex Ultimate 3000 HPLC
  • Camag TLC-MS interface (interface for thin-layer chromatograms to the mass spectrometer)
  • VWR Hitachi Chromaster HPLC (with normal and reversed phase)
  • GC-MS instrument system Perkin Elmer Clarus SQ8S
Detailed picture of the open Euler cradle on the STOE single crystal diffractometer
TUBAF

X-ray diffraction and crystal growing

  • Single crystal diffractometer STOE StadiVari with cooling device for single crystals.
  • Thermally insulated box for crystal growth using static temperature control, a temperature gradient and electric field
The picture shows a high vacuum system including a pump, Dewar vessels and various pipes and valves.
TUBAF

Synthesis technology

  • preparative HPLC (Knauer LaPrep)
  • flash chromatography system (Biotage Isolera One)
  • preparative microwave device (CEM Discover SP)
  • preparative ultrasound device (Branson Sonifer 450)
  • photochemical reactors (Peschl Ultraviolet photon Cabinet)
Section of the SPE unit. Syringes with cannulas on the robot arm.
TUBAF

Further methods of analysis

  • Jasco FP8500 fluorescence spectrometer incl. FMP825, EHC813, SHP820
  • Elementar CHN VarioMicro Cube Analyser elemental analyser
  • Thermometrics 2277 Thermal Activity Monitor microcalorimeter
  • Krüss P8000T polarimeter