Dr.-Ing. Graduations at ITUN after 2017
On August 30th, 2024, Martin Dirauf M.Sc. successfully (summa cum laude) defended his doctoral thesis entitled
“Mass transfer during biopolymer aerogel production: measurement and modeling”.
As a consequence, the title “Doktor Ingenieur” was conferred on him by the Faculty 4 on behalf of the Technische Universität Bergakademie Freiberg.
Martin Dirauf joined ITUN as doctoral researcher after he had completed the master programme “Chemie- und Bioingeneiurwesen” at Friedrich-Alexander-Universität Erlangen-Nürnberg. He contributed to several journal papers:
- M.P. Dirauf, P.C. Wagner, A.S. Braeuer
Mass transfer kinetics inside bio-(aero)gels during solvent exchange and supercritical drying: On the relevance of advection, gel-porosity and a peculiarity regarding the tortuosity
The Journal of Supercritical Fluids 191, 105762 (2022)
- F. Spiske, M.P. Dirauf, A.S. Braeuer
Aerogel-lined capillaries for Raman signal gain of aqueous mixtures
Sensors 22, 4388 (2022)
- I. Preibisch, M.P. Dirauf, T. Lehmann, P. Gurikov, A.S. Braeuer, I. Smirnova
CO2 induced gelation of amidated pectin solutions: Impact of viscosity and gel formation
Chemical Engineering Research and Design 180, 153-163 (2022)
- M.P. Dirauf, M. Conrad, A.S. Braeuer
Non-saturated mixture densities of the binary systems of carbon dioxide and the organic solvents ethanol, acetone, acetonitrile and dimethyl sulfoxide from 6-12 MPa
Fluid Phase Equilibria 549, 113201 (2021)
- M.P. Dirauf, A. Hajnal, P. Gurikov, A.S. Braeuer
Protein gel shrinkage during solvent exchange: Quantification of gel compaction, mass transfer and compressive strength
Food Hydrocolloids 120, 106916 (2021)
On August 28th, 2023, Michael Fechter M.Sc. successfully defended his doctoral thesis entitled
“Measurement of thermodynamic data at elevated pressure and temperature conditions with a microfluidic setup”.
As a consequence, the title “Doktor Ingenieur” was conferred on him by the Faculty 4 on behalf of the Technische Universität Bergakademie Freiberg.
Michael Fechter joined ITUN as doctoral researcher after he had completed the master programme “Verfahrenstechnik” at TUBAF. He contributed to several journal papers:
- M.H.H. Fechter, A.S. Braeuer
Vapor–liquid equilibria of binary systems consisting of nitrogen and n-tridecane, n-pentadecane, n-hexadecane, and n-heptadecane at pressures of 1.5–9 MPa and temperatures of 303–633 K determined with a Raman spectroscopy-coupled microfluidic device
Journal of Chemical & Engineering Data 68, 1976–1988 (2023)
- M.H.H. Fechter, J. Koschack, A.S. Braeuer
Vapor-Liquid Equilibria of the systems 1-octanol/nitrogen and 1-octanol/oxygen at pressures from 3 to 9 MPa and temperatures up to 613 K – measured in a microcapillary with Raman spectroscopy
Fuel 323, 124352 (2022)
- M.H.H. Fechter, Ph. Haspel, Ch. Hasse, A.S. Braeuer
Vapor pressures and latent heats of vaporization of Poly(oxymethylene) Dimethyl Ethers (OME3 and OME4) up to the vicinity of the critical temperature
Fuel 303, 121274 (2021)
- T. Deleau, M.H. Fechter, J.-J. Letourneau, S. Camy, J. Aubin, A.S. Braeuer, F. Espitalier
Determination of mass transfer coefficients in high-pressure two-phase flows in capillaries using Raman spectroscopy
Chemical Engineering Science 228, 115960 (2020)
- M.H.H. Fechter, A.S. Braeuer
Vapor-Liquid-Equilibria of mixtures containing ethanol, oxygen and nitrogen at elevated pressure and temperature – measured with in situ Raman spectroscopy in microcapillaries
Journal of Chemical & Engineering Data 65, 3373–3383 (2020)
- F. Grahl, N. Beitlich, M. Fechter, K. Speer, V. Herdegen, M. Eßlinger, R. Haseneder,J.‐U. Repke
New Approach for the Material Use of Press Water from Brewers' Spent Grains Using Membrane Technology
Chemie Ingenieur Technik, 91, 1–13 (2019)
On March 27th, 2023 Laura Lohmeier M.Sc. Lohmeier successfully defended her doctoral thesis entitled
“Agglomerationstechnologien für Reststoffe aus Midrex-Direktreduktionsanlagen”.
As a consequence, the title “Doktor Ingenieur” was conferred on her by the Faculty 4 on behalf of the Technische Universität Bergakademie Freiberg. Laura Lohmeier contributed to several journal papers:
- L. Lohmeier, Ch. Thaler, Ch. Harris, R. Wollenberg, H.W. Schröder, A.S. Braeuer
Use of bentonite and organic binders in the briquetting of particulate residues from the Midrex process for improving the thermal stability and reducibility of the briquettes
Steel Research International 2021, 2100210 (2021)
- L. Lohmeier, C. Thaler, C. Harris, R. Wollenberg, H.-W. Schröder
Briquetting of fine-grained residues from iron and steel production using organic and inorganic binders
Steel Research International 91, 2000238 (2020)
- L. Lohmeier, R. Wollenberg, H.-W. Schröder
Investigation into the hot briquetting of fine-grained residual materials from iron and steel production
Steel Research International 91, 2000237 (2020)
- L. Lohmeier, K. Schaldach, F. Fehse, H.-W. Schröder
ACHEMA 2018: Agglomerationstechnik auf der ACHEMA 2018
Chemie Ingenieur Technik 90, 1964–1971 (2018)
Dr.-Ing. Katja Schaldach successfully defended her doctoral dissertation on June 22nd, 2022. As a consequence, the title Dr.-Ing. was bestowed on her by the faculty 4 on behalf of the TU Bergakademie Freiberg.
The title of her thesis is “Mechanical and thermal conversion of agricultural by-products for the generation of pelletized adsorbents”.
Dr.-Ing. Katja Schaldach joined the ITUN-Team as doctoral researcher in 2015 and since has been investigating into the mechanical, thermal and chemical treatment of agricultural by-products for their conversion into pelletized adsorbents. The target was (and has been achieved) the generation of pelletized adsorbents which are competitive to commercially available pelletized activated carbons. From her research some publications resulted:
- Aktivierung und Formgebung zur Verbesserung der Eigenschaften von Adsorbentien aus Agrarreststoffen
(K. Schaldach, V. Herdegen, H.-W. Schröder, J.-U. Repke; Chemie Ingenieur Technik 89 (2017) 12, S. 1669-1678, DOI: 10.1002/cite.201700064) - Agglomerationstechnik auf der ACHEMA 2018
(L. Lohmeier, K. Schaldach, F. Fehse, H.-W. Schröder; Chemie Ingenieur Technik 90 (2018) 12, S. 1998-2003, DOI: 10.1002/cite.201800155) - A concept for an integrated process scheme for by-products from rice and sugarcane processing
(K. Schaldach, H.-W. Schröder, V. Herdegen, D. N. Vinh; Chemie Ingenieur Technik 92 (2020) 11, S. 1790-1796, DOI: 10.1002/cite.202000088) - K. Schaldach, V. Herdegen, A.S. Braeuer, Do Nang Vinh, Nguyen Van Toan, Le Van Tam „Sustainable value added material use of occurring by-products from sugar and rice production in Vietnam”
Science of the Total Environment (2022), 835, 155414,
10.1016/j.scitotenv.2022.155414
On January 17th, 2022, Medhanie Tesfay Gebrekidan M.Sc. hon. successfully defended his doctoral thesis.
As a consequence, the title “Doktor Ingenieur” was conferred on him by the Faculty 4 on behalf of the Technische Universität Bergakademie Freiberg. The title of his thesis is:
"Refinement of Raman spectra from extreme background and noise interferences – Cancer diagnostics using Raman spectroscopy"
Dr.-Ing. Gebrekidan was carrying out his research first as scholarship holder at the Erlangen-Graduate School in Advanced Optical Technologies at the Friedrich-Alexander-University Erlangen-Nürnberg, before he moved with his supervisor to the TU Bergakademie Freiberg. After the move he continued his research funded by the Wilhelm-Sander-Stiftung (Krebsforschungsförderung). Most recognizable are his achievements in the field of spectra processing using methods of artificial intelligence. As a doctoral researcher he contributed significantly to the following high-class publications:
- M.T. Gebrekidan, Ch. Knipfer, A.S. Braeuer
Raman Fiber Bundle Probe of Individually Filter-Coated Fibers
International Journal of Optics and Photonic Engineering (accepted December 2021)
- L. Matthies, M.T. Gebrekidan, J.F. Tegtmeyer, N. Oetter, M. Rohde, T. Vollkommer, R. Smeets, W. Wilczak, F. Stelzle, M. Gosau, A.S. Braeuer, Ch. Knipfer
Optical Diagnosis of Oral Cavity Lesions by label-free Raman Spectroscopy
Biomedical Optics Express 12, 836-851 (2021)
- M.T. Gebrekidan, Ch. Knipfer, A.S. Braeuer
Refinement of spectra using a deep neural network; fully automated removal of noise and background
Journal of Raman spectroscopy 52, 723-736 (2021)
- M.T. Gebrekidan, Ch. Knipfer, A.S. Braeuer
Vector casting for noise reduction
Journal of Raman Spectroscopy 51, 731–743 (2020)
- T.M. Gebrekidan, R. Erber, A. Hartmann, P.A. Fasching, J. Emons, M.W. Beckmann, A.S. Braeuer
Breast tumor analysis using Shifted-Excitation Raman Difference Spectroscopy (SERDS)
Technology in Cancer Research & Treatment 17 (2018)
- F. Michelino, M.T. Gebrekidan, A. Zambon, M. Vetralla, A. Braeuer, S. Spilimbergo
In situ Raman-analysis of supercritical carbon dioxide drying applied to acellular esophageal matrix
The Journal of Supercritical Fluids 128, 194-199 (2017)
- A.S. Braeuer, J.J. Schuster, M.T. Gebrekidan, L. Bahr, F. Michelino, A. Zambon, S. Spilimbergo
In situ Raman-analysis of CO2–assisted drying of fruit-slices
Foods 37, 6, 11 pages (2017)
- M.T. Gebrekidan, C. Knipfer, F. Stelzle, J. Popp, S. Will, A. Braeuer
A Shifted-Excitation Raman Difference Spectroscopy (SERDS) evaluation strategy for the efficient isolation of Raman spectra from extreme fluorescence interference
Journal of Raman Spectroscopy 47, 198–209 (2016)
- C. Knipfer, J. Motz, W. Adler, K. Brunner, M.T. Gebrekidan, R. Hankel, A. Agaimy, S. Will, A. Braeuer, F.W. Neukam, F. Stelzle
Raman difference spectroscopy: a non-invasive method for identification of oral squamous cell carcinoma
Biomedical Optics Express 5, 3252-3265 (2014)
On July 9th, 2021, Leo Alexander Bahr M.Sc. successfully defended his doctoral thesis.
As a consequence, the title “Doktor Ingenieur” was conferred on him by the Faculty 4 on behalf of the Technische Universität Bergakademie Freiberg. The title of his thesis is:
"Multivariate Untersuchungen in Gasphasenprozessen und Aerosolen mittels Raman-Spektroskopie"
Dr. Bahr was carrying out his main research within a DFG-funded project “Online Bestimmung der polymorphen Modifikation kristalliner Nanopartikel in der Gasphase” (Online assessment of the crystalline modification of nanoparticles in the gas phase). As a doctoral researcher he contributed significantly to the following high-class publications:
- L. A. Bahr, F.J.T. Huber, S. Will, A.S. Braeuer
Shifted-excitation rotational Raman spectroscopy and Bayesian inference for in situ temperature and composition determination in laminar flames
Journal of Quantitative Spectroscopy and Radiative Transfer 249, 106996 (2020)
- A. Roßbach, L.A. Bahr, S. Gäbel, A.S. Braeuer, A. Wierschem
Growth rate of pressure induced triolein crystals
American Oil Chemists Society 96, 25-33 (2019)
- L.A. Bahr, T. Dousset, S. Will, A.S. Braeuer
In situ analysis of aerosols by Raman spectroscopy – crystalline particle polymorphism and gas-phase temperature
Journal of Aerosol Science 126, 143-151 (2018)
- L.A. Bahr, P. Fendt, Y. Pang, J. Karl, T. Hammer, A.S. Braeuer, S. Will
Temperature determination of superheated water vapor by rotational-vibrational Raman spectroscopy
Optics Letters 43, 4477-4480 (2018)
- J.J. Schuster, L.A. Bahr, L. Fehr, M. Tippelt, J. Schulmeyr, A. Wuzik, A.S. Braeuer
Online monitoring of the supercritical CO2 extraction of hop
The Journal of Supercritical Fluids 133, 139-145 (2018)
- A.S. Braeuer, J.J. Schuster, M.T. Gebrekidan, L. Bahr, F. Michelino, A. Zambon, S. Spilimbergo
In situ Raman-analysis of CO2–assisted drying of fruit-slices
Foods 37, 6, 11 pages (2017)
Simon Stehle M.Sc. promoted to Doctor in Engineering (Dr.-Ing)
On November 20th, 2020, Simon Stehle M.Sc. successfully defended his Doctoral thesis. As a consequence the title "Doktor Ingenieur" was conferred on him by the Faculty 4 on behalf of the Technische Universität Bergakademie Freiberg. The title of his thesis is:
"Raman spektroskopische Untersuchung von einphasigen strukturierten Stoffgemischen in einem Mikrokapillarsystem (Investigations into single-phase structured fluid systems in micro-capillaries using Raman spectroscopy)"
Doctor Stehle was carrying out his research within the frame of an ERC Starting grant project "Inhomogeneities" (637654). As a doctoral researcher he contributed significantly to the following high-class publications:
- S. Stehle, E. Nemati Lay, A. Triolo, N. Ventosa, A.S. Braeuer
A fast and remote screening method for sub-micro-structuration in pressurized mixtures containing water and carbon dioxide
The Journal of Supercritical Fluids 152, 104555 (2019)
- S. Stehle, A.S. Braeuer
Hydrogen Bond Networks in Binary Mixtures of Water and Organic Solvent
The Journal of Physical Chemistry B 123, 4425-4433 (2019)
- N. Grimaldi, P.E. Rojas, S. Stehle, A. Cordoba, R. Schweins, S. Sala, S. Luelsdorf, D. Piña, J. Veciana, J. Faraudo, A. Triolo, A.S. Braeuer, N. Ventosa
Pressure-responsive, surfactant-free CO2-based nanostructured fluids
ACS Nano 11, 10774–10784 (2017)
- S.K. Luther, S. Stehle, K. Weihs, S.Will, A. Braeuer
Determination of vapor-liquid equilibrium data in microfluidic segmented flows at elevated pressures using Raman spectroscopy
Analytical Chemistry 87, 8165–8172 (2015)
Dr. Stehle has been working for Eisenbau Heilbronn since April 2019
Julian Schuster M.Sc. promoted to Doctor in Engineering (Dr.-Ing)
On March 6th, 2020, Julin Schuster M.Sc. successfully defended his Doctoral thesis. As a consequence the title "Doktor Ingenieur" was conferred on him by the Friedrich-Alexader-Universität Erlangen-Nürnberg. The title of his thesis is:
"Insights into near-critical and supercritical fluid technologies for the treatment of food using Raman spectroscopy"
As a doctoral researcher he contributed significantly to the following high-class publications:
- J.J. Schuster, L.A. Bahr, L. Fehr, M. Tippelt, J. Schulmeyr, A. Wuzik, A.S. Braeuer
Online monitoring of the supercritical CO2 extraction of hop
The Journal of Supercritical Fluids 133, 139-145 (2018)
- A.S. Braeuer, J.J. Schuster, M.T. Gebrekidan, L. Bahr, F. Michelino, A. Zambon, S. Spilimbergo
In situ Raman-analysis of CO2–assisted drying of fruit-slices
Foods 37, 6, 11 pages (2017)
- V. Strobel, J.J. Schuster, A.S. Braeuer, L. Vogt, H. Junge, M. Haumann
Shining light onto the low-temperature methanol aqueous-phase reforming using homogeneous Ru-pincer complexes – operando Raman-GC studies
Reaction Chemistry & Engineering 2, 390-396 (2017)
- G. Ferrentino, J.J. Schuster, A. Braeuer, S. Spilimbergo
In situ Raman quantification of the dissolution kinetics of carbon dioxide in liquid solutions during a dense phase and ultrasound treatment for the inactivation of Saccharomyces cerevisiae
The Journal of Supercritical Fluids 111, 104-111 (2016)
- J.J. Schuster, Ph. Siegler, A. Guenther, K.-E. Wirth, A. Braeuer
Simultaneous analysis of the dispersed liquid and the bulk gas phase of water sprays using Raman spectroscopy
Applied Spectroscopy 70, 1055-1062 (2016)
- A. Braeuer, R. F. Hankel, M. K. Mehnert, J.J. Schuster, S. Will
A Raman technique applicable for the analysis of the working principle of promoters and inhibitors of gas hydrate formation
Journal of Raman Spectroscopy 46, 1145-1149 (2015)
- J. J. Schuster, S. Will, A. Leipertz, A. Braeuer
Deconvolution of Raman spectra for the quantification of ternary high pressure phase equilibria composed of carbon dioxide, water and organic solvent
Journal of Raman Spectroscopy 45, 246-252 (2014) - S.K. Luther, J.J. Schuster, A. Leipertz, A. Braeuer
Microfluidic investigation into mass transfer in compressible multi-phase systems composed of oil, water and carbon dioxide at elevated pressure
The Journal of Supercritical Fluids 84, 121-131 (2013)
- S. K. Luther, J. J. Schuster, A. Leipertz, A. Braeuer
Non-invasive quantification of phase equilibria of ternary mixtures composed of carbon dioxide, organic solvent and water
The Journal of Supercritical Fluids 84, 146-154 (2013)
- R. Adami, J. J. Schuster, S. Liparoti, E. Reverchon, A. Leipertz, A. Braeuer
A Raman spectroscopic method for determining vapour liquid equilibria
Fluid Phase Equilibria 360, 265-273 (2013)
Dr. Schuster has been working for Linde Gas since August 2018.
Tobias Klima M.Sc. promoted to Doctor in Engineering (Dr.-Ing)
On December 17th, 2019, Tobias Klima M.Sc. successfully defended his Doctoral thesis. As a consequence the title "Doktor Ingenieur" was conferred on him by the Faculty 4 on behalf of the Technische Universität Bergakademie Freiberg. The title of his thesis is:
"Quantitative insights into the transcritical mixture formation at diesel relevant conditions"
Doctor Klima was carrying out his research within the frame of an ERC Starting grant project "Inhomogeneities" (637654). As a doctoral researcher he contributed significantly to the following high-class publications:
- T.C. Klima, A. Peter, S. Riess, M. Wensing, A.S. Braeuer
Quantification of mixture composition, liquid-phase fraction and - temperature in transcritical sprays
The Journal of Supercritical Fluids 159, 104777 (2020)
- T.C. Klima, A.S. Braeuer
Raman thermometry in water, ethanol and ethanol/nitrogen-mixtures from ambient to critical conditions
Analytical Chemistry 91, 1043-1048 (2019)
- T.C. Klima, A.S. Braeuer
Vapor-Liquid-Equilibria of Fuel-Nitrogen Systems at Engine-like Conditions measured with Raman spectroscopy in micro capillaries
Fuel 238, 312-319 (2019)
- J. Quiño, M. Rühl, T. Klima, F. Ruiz, S. Will, A. Braeuer Supercritical drying of aerogel: In situ analysis of concentration profiles inside the gel and derivation of the effective binary diffusion coefficient using Raman spectroscopy The Journal of Supercritical Fluids 108, 1-12 (2016)
B. Münsterjohann, F.J.T. Huber, T.C. Klima, S. Holfelder, S.R. Engel, J.D. Miller, T.R. Meyer, S. Will
Potential of two-line atomic fluorescence for temperature imaging in turbulent indium-oxide-producing flames
Journal of Nanoparticle Research 17, 459 (2015)
Dr. Klima has been working for Diehl Defence since November 2018.
On October 18th, 2019, Christine Holzammer M.Sc. successfully defended her Doctoral thesis. As a consequence the title "Doctor Ingenieurin" was conferred on her by the Faculty 4 on behalf of the Technische Universität Bergakademie Freiberg. The title of her thesis is:
"Raman Spectroscopic Study of the Effect of Aqueous Salt Solutions on the Formation and Dissociation Behavior of CO2 Gas Hydrates"
Doctor Holzammer was carrying out her research within the frame of an ERC Starting grant project "Inhomogeneities" (637654). As a doctoral researcher she contributed significantly to the following high-class publications:
- Ch. C. Holzammer, A.S. Braeuer
Raman spectroscopic study of the effect of aqueous salt solutions on the inhibition of carbon dioxide gas hydrates
The Journal of Physical Chemistry B 123, 2354-2361 (2019)
- Ch. Holzammer, J. Schicks, S. Will, A.S. Braeuer
Influence of Sodium Chloride on the Formation and Dissociation Behavior of CO2 Gas Hydrates
The Journal of Physical Chemistry B 121, 8330-8337 (2017)
- Ch. Holzammer, A. Finckenstein, S. Will, A. Braeuer
How Sodium Chloride Salt Inhibits the Formation of CO2 Gas Hydrates
The Journal of Physical Chemistry B 120, 2452–2459 (2016)
- G. Lipinski, Ch. Holzammer, M. Petermann, M. Richter
Measurement of sorption phenomena near dew points of fluid mixtures: concept for the combination of gravimetric sorption analysis and Raman spectroscopy
Measurement Science and Technology 29, 105501-105506 (2018)
Dr. Holzammer has been working for BASF since July 2019.
Dr.-Ing. Arite Werner defended her doctoral examination successfully on November 23rd, 2018.
The title of her doctoral thesis is:
"Entwicklung eines membranbasierten Trenn- und Anreicherungsverfahrens zur selektiven Gewinnung von Indium und Germanium aus Laugungslösungen"
The elements indium and germanium are among the economic-strategic elements due to the steadily rising demand and the strong fixation on the nearly sole producer China. Against this background, an alternative method of biohydrometallurgical recovery was investigated at the 2nd Krüger Research College. The focus of this work is the selective separation of indium and germanium from complex model solutions through the application of nanofiltration. By developing a systematic methodology, the pH-dependent separation behaviour of the target elements, with variation of the process parameters and the process control, was specifically investigated. The variation of the pH allows the selective separation of indium and germanium from the model solutions. The transferability to real concentration ratios was successfully implemented by indium enriched in the retentate and germanium was selectively separated with the permeate.
Dr.-Ing. Franz Fehse defended his doctoral examination successfully on June 1st, 2018.
The title of his thesis is “Granulierung von Weichbraunkohle für die stoffliche Nutzung” (Granulation of brown coal for material usage)".
For the material usage of brown coal the mechanical refinement of the coal is an important process step. One example is the production of granules from brown coal with a narrow particle size distribution and high mechanical strength.
In the thesis the granulation of a brown coal from Central Germany was systematically investigated using different procedural approaches. One of the approaches used an intensive mixer for granulation of the coal. In laboratory-scale investigations the influence of the different process and machine parameters was determined independently. Using different sizes of mixers the scale-up behaviour of the granulation process was determined successfully. Thereby it is possible to produce high-quality granules with customised properties e. g. for montan-wax extraction or gas purification.