Details

Dr. rer. nat. Philipp Rathsack

Dr. rer. nat. Philipp Rathsack


Group thermochemical conversion

Zimmer DBI 210

Telefon +49 (0) 3731 39 4483
Philipp [dot] Rathsackatextern [dot] tu-freiberg [dot] de



Background
2001 - 2007Studies in Chemistry (Diploma) at TU Bergakademie Freiberg
Diploma thesis: „Limits of ESI-MS during protein species analysis“
2007 - 2018Research associate at Institute of Analytical Chemistry, TU Bergakademie Freiberg
2007 - 2009Research associate in project „Advanced Water Treatment as a Key Element to Enable Green Mining“ and „Trace elements in acid mine drainage“ (Siemens AG)
2009 - 2014Research associate in project „German centre for energy resources (DER)“ (FKZ 03IS2021A)
Field of work: Qualitative and quantitative analysis of pyrolysis liquids from coal using GCxGC-MS and FT-ICR-MS
2015PhD thesis at TU Bergakademie Freiberg (Dr. rer. nat) „Analysis of organic compounds in pyrolysis liquids by high resolving chromatographic and mass spectrometric analytical methods“
2015 - 2018Research associate in project „Winning of economically strategic materials from fine-grained residues from copper smelting - Theisenschlamm“ (FKZ 033R137)
Field of work: Qualitative and quantitative analysis of the organic components in Theisenschlamm by means of highly resolving analytical methods
02/2018 - 07/2018Research associate at IEC, Chair of Energy Process Engineering and Thermal Waste Treatment, TU Bergakademie Freiberg
Since 08/2018Research associate at Fraunhofer Institute for Microstructure of Materials and Systems IMWS, Circular Carbon Technologies
Research topics
  • Analysis of highly complex mixtures of organic compounds like oils and tars from pyrolysis by chromatographic and mass spectrometric methods
  • Application of chemometric data evaluation methods for unravelling complex datasets from different analytical methods
Publications

Peer reviewed articles

Zuber, J., Rathsack, P., Otto, M. 2018. Structural Characterization of Acidic Compounds in Pyrolysis Liquids Using Collision-Induced Dissociation and Fourier Transform Ion Cyclotron Resonance Mass Spectrometry. Analytical Chemistry, (2018), revised and submitted.

Dittrich, N., Zuber, J., Rathsack, P., Otto, M. 2018. Comparison of graphite-assisted laser desorption/ionization and matrix-assisted laser desorption/ionization Fourier transform ion cyclotron resonance mass spectrometry for the analysis of pyrolysis liquids. International Journal of Mass Spectrometry, (2018), pp. 31-39.

Dittrich, N., Zuber, J., Rathsack, P. 2018. Screening of organic compounds in complexly contaminated scrubber dust by GCxGC-MS and FT-ICR-MS. Microchemical Journal, 139 (2018), pp. 85-93.

Zuber, J., Rathsack, P., Otto, M. 2017. Characterization of a pyrolysis liquid from a German brown coal by use of negative and positive ion mode electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry and collision-induced dissociation. Fuel, 200 (2017), pp. 113-123.

Rathsack, P. 2017. Analysis of pyrolysis liquids obtained from the slow pyrolysis of a german brown coal by comprehensive gas chromatography mass spectrometry. Fuel, 191 (2017), pp. 312-321.

Zuber, J., Kroll, M. M., Rathsack, P., Otto, M. 2016. Gas Chromatography/Atmospheric Pressure Chemical Ionization-Fourier Transform Ion Cyclotron Resonance Mass Spectrometry of Pyrolysis Oil from German Brown Coal. International Journal of Analytical Chemistry 2016, 3 (2016), pp. 1-12.

Rathsack, P., Riedewald, F., Sousa-Gallagher, M. 2015. Analysis of pyrolysis liquid obtained from whole tyre pyrolysis with molten zinc as the heat transfer media using comprehensive gas chromatography mass spectrometry. Journal of Analytical and Applied Pyrolysis, 116 (2015), pp. 49-57.

Rathsack, P., Wolf, B., Kroll, M. M., Otto, M. 2015. Comparative Study of Graphite-Supported LDI- and ESI-FT-ICR-MS of a Pyrolysis Liquid from a German Brown Coal. Analytical Chemistry 87, 15 (2015), pp. 7618-7627.

Rathsack, P., Rieger, A., Haseneder, R., Gerlach, D., Repke, J.-U., Otto, M. 2014. Analysis of pyrolysis liquids from scrap tires using comprehensive gas chromatography mass spectrometry and unsupervised learning. Journal of Analytical and Applied Pyrolysis, 109 (2014), pp. 234-243.

Rathsack, P., Reichel, D., Krzack, S., Otto, M. 2014. Komprehensive Gaschromatographie Massenspektrometrie von Alkylbenzenen in Pyrolyseölen aus Biomasse und Kohle. Chemie Ingenieur Technik 86, 10 (2014), pp. 1779-1789.

Rathsack, P., Kroll, M. M., Rieger, A., Haseneder, R., Gerlach, D., Repke, J.-U., Otto, M. 2014. Analysis of high molecular weight compounds in pyrolysis liquids from scrap tires using fourier transform ion cyclotron resonance mass spectrometry. Journal of Analytical and Applied Pyrolysis, 107 (2014), pp. 142-149.

Rathsack, P., Kroll, M. M., Otto, M. 2014. Analysis of high molecular compounds in pyrolysis liquids from a german brown coal by FT-ICR-MS. Fuel, 115 (2014), pp. 461-468.

Rathsack, P., Otto, M. 2014. Classification of chemical compound classes in slow pyrolysis liquids from brown coal using comprehensive gas-chromatography mass-spectrometry. Fuel, 116 (2014), pp. 841-849.

 

Presentations and posters

Rathsack. P. (2016). Analysis of complex mixtures of organic compounds from coal or tyre pyrolysis by GCxGC-MS. 40th International Symposium on Capillary Chromatography and 13th GCxGC Symposium, Riva del Garda, Italy, 2016.

Rathsack, P., Kroll, M. M., Otto, M. 2015. Analysis of pyrolysis liquids from coal or scrap tires by graphite assisted laser desorption ultra high resolution mass spectrometry. 5th German-Japanese Joint Symposium “Development and Technology of Carbon Materials”, Freiberg, Germany, 2015.

Rathsack, P., Otto, M. 2014. Analysis of pyrolysis liquids by comprehensive gas chromatography mass spectrometry GCxGC-MS. 38th International Symposium on Capillary Chromatography and 11th GCxGC Symposium, Riva del Garda, Italy, 2014.

Otto, M., Rathsack, P., Hübler, C. 2013. Classification and prediction methods for comprehensive gas chromatography mass spectrometry. 8th CCM – Colloquium Chemiometricum Mediterraneum, Bevagna, Italy, 2013.

Rathsack, P., Kroll, M. M., Otto, M. 2012. Analysis of pyrolysis oils of coal by high performance analytical methods. 29th International Pittsburgh Coal Conference, Pittsburgh, USA, 2012.

Rathsack, P., Otto, M. 2012. Analysis of pyrolysis oils from biomass or coal by comprehensive gas-chromatography mass-spectrometry. 5th International Freiberg Conference on IGCC & XtL Technologies, Leipzig, Germany, 2012.

Rathsack, P., Otto, M. 2011. Analytik von Pyrolyseölen aus Biomasse und Kohle. Anwendertreffen Separation Science, Mönchengladbach, Germany, 2011.

Rathsack, P., Otto, M. 2010. Analysis of pyrolysis products from biomass and coal by comprehensive two-dimensional gas-chromatography. (Poster) 28th International Symposium on Chromatography, Valencia, Spain, 2010.

Rathsack, P., Otto, M. 2009. Application of capillary electrophoresis for mine water analysis. Berg- und Hüttenmännischer Tag, Freiberg, Germany, 2009.

 

Patents

Klein, R., Schlömann, M., Mühling, M., Glombitza, F., Janneck, E., Otto, M., Rathsack, P. 2014. Behandlung von Abwässern, insbesondere von sulfat- und/oder schwermetallhaltigen Minenwässern. Angemeldet durch Siemens AG. Veröffentlichungsnr: WO 2014037276 A2, 2014.

 

Book chapters and conference proceedings

Kroll, M. M., Schmidt, M., Brendler, E., Bauer, D., Rathsack, P., Wolf, B., Otto, M. 2013. Ionenzyklotron- und kernmagnetische Resonanz-Spektrometrie zur Kohleanalytik. ACAMONTA – Zeitschrift für Freunde und Förderer der Technischen Universität Bergakademie Freiberg, 20 (2013), pp. 54-57.

Kroll, M., Bauer, D., Wolf, B., Rathsack, P., Otto, M. 2012. Schwarzes Gold - Kohle und Biomasse unter der Ultra-Hochauflösungslupe FT-ICR-MS. labor&more 4 (2012), pp. 32-35.

Otto, M., Bauer, D., Rathsack, P., Schmidt, M. 2012. Hochleistungsanalytik für Energierohstoffe. ACAMONTA - Zeitschrift für Freunde und Förderer der Technischen Universität Bergakademie Freiberg, 19 (2012), pp. 18-21.

Otto, M., Bauer, D., Rathsack, P., Reichel, D., Schmidt, M. 2011. Strukturaufklärung von Energierohstoffen. Kraftwerkstechnik Band 3: Sichere und nachhaltige Energieversorgung, Beiträge des 43. Kraftwerkstechnischen Kolloquiums, TK Verlag (2011), pp. 623-633.